- 제조사:
- BEL Japan, Inc.
- 키워드:
- 비표면적 (BET surface area),금속분산도 (Metal Dispersion Rate),촉매특성평가 (TPD/TPR/TPO),부피식흡착 (volumatric sorption),화학흡착 (chemisorption),물리흡착 (physisorption)
Automatic gas and vapor adsorption analyzer
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OVERVIEW
The BELSORP-max is designed for wide range adsorption isotherm for surface area and pore size distribution analysis. It can measure adsorption isotherms from relative pressure as low as 1 x10-8 (N2 at 77K, Ar at 87K), using a 13.3Pa pressure transducer. Also AFSM, the new method for free space measurement, is applied and adsorption isotherm can be measured with high accuracy. Chemisorption option enables unattended chemisorption measurement from pretreatment with step programs.
FEATURES
-Specific surface area, pore size distribution, vapor adsorption and chemisorption (OP) can be measured. -Adsorption measurement from extremely low pressure (p/po=10-8 - 0.997) -Up to 3 samples can be measured simultaneously. -Fully automated chemisorption option is available.- Kr adsorption is available for low surface area material. -Coolant level controller is no longer necessary and high reproducible data can be obtained (AFSM). -BELSim, which analyze the pore size distribution by NLDFT and GCMC simulation method can be incorporated into the powerful data analysis software, BELMaster. -ISO 9277 and JIS Z 8830 compliant
SPECIFICATION
Measuring principle |
Volumetric gas adsorption method+AFSM |
Adsorptive |
N2, Ar, Kr, NH3, CO2, H2, CO, O2, CH4 and other non-corrosive gases H2O, MeOH, EtOH, C6H6 and other non-corrosive vapor |
Analysis port |
STD mode (p/p0=10-4 - 0.997) 3 ports High accuracy mode (p/p0=10-4 - 0.997) 2 ports High accuracy mode (p/p0=10-8 - 0.997) 1 port (OP : 2 ports) |
Specific surface area |
0.01m2/g and above (N2/77K) 0.0005 m2/g and above (Kr/77K) |
Pore size distribution |
0.32 - 500 nm in pore diameter |
Pressure transducer |
133 kPa (1000Torr) 0.5 % of F.S. 5 units 1.33kPa (10Torr) 0.5% of R. 2 units (OP : 3 units) 0.0133kPa (0.1Torr) 0.15% of R. 1 units (OP : 2 units) |
Thermostated air oven |
40oC |
Dewar vessel |
Volume 2.6L Holding time 60H |
Sample cell |
Approx. 1.8cm3 (Option: 5 cm3) |
Vacuum pump |
Turbo molecular drug pump + Fore vacuum pump(OP) Ultimate vacuum: 6.7 x 10-7 Pa and below |
Vacuum gauge |
Pirani + Cold cathode gauge (ATM - 5x10-7 Pa) |
Physical |
W565 x H850 x D580 mm, 84 kg (Not includes vacuum pump, computer and its peripheral) |
Power |
Single phase: AC100-120V or 200-240V / 1500VA (400VA is for vacuum pump) |
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